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The pyrolysis mass spectra of 1 : 1 (alt.), 1 : 1 (random), 3 : 1 and 1 : 3 PEK/PES copolymers appear essentially identical (apart for obvious differences in peak intensities), indicating that the molecular rearrangements (SO2 extrusion, transesterification, cleavage of bridges) which occur at higher temperatures and/or in the pyrolysis processes are able to randomize the distribution of comonomer units originally present in the copolymers